英语翻译This example provides an example of a small-scale crystallization of Forn I the besylate salt of compound 101 from the free base of compound 101.Compound 101 was recrystallized as Form I with benzenesulfonic acid (PhSO3H-xH2O;Aldrich).3.9

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英语翻译Thisexampleprovidesanexampleofasmall-scalecrystallizationofFornIthebesylatesaltofcompound101from

英语翻译This example provides an example of a small-scale crystallization of Forn I the besylate salt of compound 101 from the free base of compound 101.Compound 101 was recrystallized as Form I with benzenesulfonic acid (PhSO3H-xH2O;Aldrich).3.9
英语翻译
This example provides an example of a small-scale crystallization of Forn I the besylate salt of compound 101 from the free base of compound 101.Compound 101 was recrystallized as Form I with benzenesulfonic acid (PhSO3H-xH2O;Aldrich).3.9g benzenesulfonic acid was dissolved in 5 ml ethanol,and this ethanol solution was added to 5.02g solid free base compound101.For this example,compound 101 was prepared according to Example 1,except that an SnCl2 reduction was used for reduction of compoundⅡto compound Ⅲ.The mixture was rinsed with 5 ml ethanol,and additional ethanol was further added to a total of 25 ml.The mixture was heated to form a complete solution and then slowly cooled with stirring.Solid Form I,5.57g,was collected by filtration and rinsed with ethanol.

英语翻译This example provides an example of a small-scale crystallization of Forn I the besylate salt of compound 101 from the free base of compound 101.Compound 101 was recrystallized as Form I with benzenesulfonic acid (PhSO3H-xH2O;Aldrich).3.9
请先检查一下英文文段的正确性.前两句话好像有问题,单词拼写有误,语法不通.（我不是学化工的,只能根据字面意思翻译,如有错误,请见谅.）
这个样本提供了一个从101号化合物自由基中提取少量1型苯磺酸盐结晶的范例.当与苯磺酸钠反应,101号化合物就再度结晶为1型物质.(PhSO3H-xH2O;Aldrich).将3.9克苯磺酸钠溶解在5毫升酒精中,再将该酒精溶液添加到5.02克固体101号化合物自由基中.对于这个样本来说,除了有一个氯化亚锡的还原反应是为了将2号化合物还原为3号化合物,101号化合物都是为1号样本准备的.用5毫升酒精冲洗混合物,额外使用的酒精量总计25毫升.将混合物加热,使其完全溶解,再缓慢搅动使其冷却.过滤,并用酒精冲洗,5.57克的1型结晶就提取完成了.

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这个例子提供了一个对福尔内小规模的结晶我的地平从复合101.Compound 101自由基地101复合结晶盐的例子是与苯磺酸作为表格I（PhSO3H - xH2O的;秩序）。 3.9G的苯磺酸溶解于5毫升乙醇，这种乙醇溶液加入五点零二克坚实的自由的基础compound101.For这个例子中，
化合物101准备根据例1，除了减少了氯化亚锡化合物Ⅱ为减少使用复合Ⅲ。混合物的5毫升乙醇冲洗，并进一步增加乙醇添加到总数的25毫升。该混合物加热，形成一个完整的解决方案，然后慢慢搅拌冷却。固体表格I，5.57克，收集了过滤，乙醇冲洗。（不知道你满不满意啊~）

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