求翻译,希望大家帮忙.不要工具翻的,谢谢啦!In a flask fitted with a reflux condenser were added 1.00 g(10.4 mmol) of 1,2-dimethylimidazole and 1.43 g (10.4 mmol)of butyl bromide. After addition, the mixture was stirred at140 ◦C d

求翻译,希望大家帮忙.不要工具翻的,谢谢啦!In a flask fitted with a reflux condenser were added 1.00 g(10.4 mmol) of 1,2-dimethylimidazole and 1.43 g (10.4 mmol)of butyl bromide. After addition, the mixture was stirred at140 ◦C d
求翻译,希望大家帮忙.不要工具翻的,谢谢啦!
In a flask fitted with a reflux condenser were added 1.00 g
(10.4 mmol) of 1,2-dimethylimidazole and 1.43 g (10.4 mmol)
of butyl bromide. After addition, the mixture was stirred at
140 ◦C during 1 h to give a white solid. This solid was recrystallized
from acetonitrile and dried under reduced pressure to give
2.29 g (95% yield) of BMMIBr as white crystals. In another
flask, 250 mg (1.07 mmol) of BMMIBr were placed and dissolved
in 5.0mL of water followed by an aqueous solution
of LiTFSI (308 mg, 1.07 mmol) in 5.0mL of water. The reaction
mixture was stirred overnight at room temperature and two
phases were formed and separated. The phase containing the
ionic liquid was washed several times with water, treated with
activated carbon and subjected to a chromatography column
(alumina, dichloromethane). The ionic liquid was dried under
reduced pressure during 3 days at 100 ◦C to give BMMITFSI as
a colorless liquid (301 mg, 0.70 mmol, 65% yield).
BMPTFSI and BMITFSI were also synthesized following
the above procedure. BMIBr was obtained as a white solid after
recrystallization from tetrahydrofuran instead of acetonitrile. All
ionic liquids were stored in an argon atmosphere glove-box Labmaster
130 (H2OandO2 < 1 ppm) and all samples were prepared
and sealed in the glove-box to avoid water contamination. The
water contain of both RTILs was measured using the standard
Karl–Fischer method and it was estimated to be below 30 ppm.
The structures of the bromide derivatives and of the ionic liquids
were identified by 1H and 13C NMR, FTIR and elemental
analysis. The results for BMMI and BMP salts are summarized
below. The BMITFSI data are not shown here due to extensive
literature data available [64–68]. It is important to note that the
yields obtained in both cases are lower than those reported by
Appetecchi et al. [69]. These differences could be assigned to
the use of bromide instead of iodine derivatives and also to the
loss of material during the purification processes.
BMMIBr data—mp 95–97 ◦C; found: C, 46.22; H, 6.96.
Calc for C9H17BrN2: C, 46.36; H, 7.35; νmax(KBr), cm−1:
3129, 3078, 2961, 2933, 2873, 1588, 1538, 1517, 1466, 1380,
1251 and 1136; δH (300 MHz, CDCl3, ppm): 0.97 (3H, t,
CH2CH2CH2CH3, J = 7 Hz), 1.40 (2H, m, CH2CH2CH2CH3),
1.81 (2H, m, CH2CH2CH2CH3), 2.83 (3H, s, CH3), 4.04 (3H,
s, NCH3), 4.25 (2H, t, CH2CH2CH2CH3, J = 7 Hz), 7.58 (1H,
d, CHring, J = 2.1 Hz) and 7.77 (1H, d, CHring, J = 2.1 Hz); δC
(75 MHz, CDCl3, ppm): 11.0, 13.6, 19.6, 31.8, 36.2, 48.8, 121.3,
123.1 and 143.7.
如果用软件翻译的麻烦别贴啦!
谢谢啦!

求翻译,希望大家帮忙.不要工具翻的,谢谢啦!In a flask fitted with a reflux condenser were added 1.00 g(10.4 mmol) of 1,2-dimethylimidazole and 1.43 g (10.4 mmol)of butyl bromide. After addition, the mixture was stirred at140 ◦C d
在一个瓶子带有回流冷凝器增加了一点○○克
（ 10.4 mmol ） 1,2 -d imethylimidazole和一点四三克（ 1 0.4m mol）
丁基溴化.之后,此外,混合搅拌,在
140 ◦ c在1 h后给予一个白色固体.这是固体结晶
从乙腈和干果的压力下,减少给
2.29克（ 95 ％收益率）的bmmibr为白色结晶物.在另一
瓶,250毫克（ 1.07 mmol ） bmmibr放置和解散
在5.0毫升水其次是一水溶液
对litfsi （ 308毫克,1.07 mmol ）在五点○毫升的水.反应
混合搅拌通宵在室温和2
分阶段形成和失散.第一阶段载
离子液体洗涤多次与水,治疗
活性炭和受到了层析柱
（氧化铝,二氯甲烷） .离子液体是干下
减少压力,在3天在100 ◦ C至给予bmmitfsi作为
无色液体,（ 301毫克,0.70 mmol ,65 ％的收益率） .
bmptfsi和bmitfsi还合成了以下
上述程序.bmibr ,获得了作为一个白色固体后
结晶从四氢呋喃,而非乙腈.全部
离子液体被存放在一氩气氛手套盒labmaster
130 （ h2oando2 < 1 ppm的）和所有样本准备
和密封在手套盒,以避免水体污染.那个
水包含双方的rtils测量使用标准
卡尔-费希尔的方法和据估计将低于30 ppm的.
结构的溴化衍生物和离子液体
确定了1H和13C NMR谱,红外光谱和元素
分析.结果bmmi和BMP盐概述
在…下面.该bmitfsi数据没有在这里显示,由于广泛
文献资料提供[ 64-68段] .这是很重要的值得注意的是,
产量得到了在这两种情况下均低于报道
阿佩泰基等人.[ 69 ] .这些分歧是可以被分配到
使用甲基溴而不是碘衍生物,也向
损失的材料在净化过程.
bmmibr数据国会议员95-97 ◦ C组发现中：C ,46.22 ; h后,6.96 .
钙为c9h17brn2中：C ,46.36 ; h后,7.35 ; ν最高（溴化钾） ,厘米- 1 ：
3129 ,3078 ,2961 ,2933 ,2873 ,1588 ,1538 ,1517 ,1466 ,1380 ,
1251年和1136年; δ H （上300 MHz的,cdcl3 ,百万分之一） ：0.97 （ 3小时,吨,
ch2ch2ch2ch3 ,j = 7赫兹） ,1.40 （ 2小时,男,ch2ch2ch2ch3 ） ,
1.81 （ 2小时,男,ch2ch2ch2ch3 ） ,2.83 （ 3小时,硫,甲基） ,4.04 （ 3小时,
s ,nch3 ） ,4.25 （ 2小时,吨,ch2ch2ch2ch3 ,j = 7赫兹） ,7.58 （ 1小时,
发展,chring ,j = 2.1赫兹）和7.77 （ 1小时,发展,chring ,j = 2.1赫兹） ; δ c
（ 75兆赫,cdcl3 ,百万分之一） ：11.0 ,13.6 ,19.6 ,31.8 ,36.2 ,48.8 ,121.3 ,
123.1和143.7 .