英语翻译Test method:Determination by Gas Chromatogrphy-Mass Selective Detection(GC-MSD)and confirmation by HighPerformance Liquid Chromatographic Analysis (HPLC/DAD)(QMA36.105.11HG)……With reference to §64LFGB B82.02-2Requirement:According to

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英语翻译Testmethod:DeterminationbyGasChromatogrphy-MassSelectiveDetection(GC-MSD)andconfirmationbyHighPe

英语翻译Test method:Determination by Gas Chromatogrphy-Mass Selective Detection(GC-MSD)and confirmation by HighPerformance Liquid Chromatographic Analysis (HPLC/DAD)(QMA36.105.11HG)……With reference to §64LFGB B82.02-2Requirement:According to
英语翻译
Test method:Determination by Gas Chromatogrphy-Mass Selective Detection(GC-MSD)and confirmation by HighPerformance Liquid Chromatographic Analysis (HPLC/DAD)(QMA36.105.11HG)……
With reference to §64LFGB B82.02-2
Requirement:According to Directive 2002/61/EC max.30 mg/kg in dyed textiles or leathers,This limit is safely kept if the concectration of banned amines in the destuff is not above 150 mg/kg
4-Aminobiphenyl\x0592-67-1\x05mg/kg\x05ND
4,4＇-Benzidine\x0592-87-5\x05mg/kg\x05ND
4-Chloro-2-methylaniline\x0595-69-2\x05mg/kg\x05ND
2-Naphthylamine\x0591-59-8\x05mg/kg\x05ND
0-Aminoazotoluene1\x0597-56-3\x05mg/kg\x05ND
5-Nitro-o-toluidine2\x0599-55-8\x05mg/kg\x05ND
4-Chloroaniline\x05106-47-8\x05mg/kg\x05ND
4-Methyoxy-1.3-phenylenediamine\x05615-05-4\x05mg/kg\x05ND
Bis-(4-aminepheny)methane\x05101-77-9\x05mg/kg\x05ND
3,3＇-Dichlorobenzidine\x0591-94-1\x05mg/kg\x05ND
3,3＇-Dimethoxybenzidine\x05119-90-4\x05mg/kg\x05ND
0-Tolidine\x05119-93-7\x05mg/kg\x05ND
3,3＇-Dimethyl-4,4＇-diaminadiphenylmethane\x05838-88-0\x05mg/kg\x05ND
2-Methoxy-5-methylaniline\x05120-71-8\x05mg/kg\x05ND
4,4＇-Methylene bis(o-chloroaniline)\x05101-14-4\x05mg/kg\x05ND
4,4＇-Oxydianiline\x05101-80-4\x05mg/kg\x05ND
4,4＇-Thiodianiline\x05139-65-1\x05mg/kg\x05ND
O-Toluidine\x0595-53-4\x05mg/kg\x05ND
2,4-Diaminotoluene\x0595-80-7\x05mg/kg\x05ND
2,4,5-Tnmethylaniline\x05137-17-7\x05mg/kg\x05ND
O-Anisidine\x0590-04-0\x05mg/kg\x05ND
4-Amino-azobenzene\x051960-9-3\x05mg/kg\x05ND
2,4-Dimethylaniline\x0595-68-1\x05mg/kg\x05ND
2,6-Dimethylaniline\x0567-62-7\x05mg/kg\x05ND
Remarks
ND :NOT detected less than 50 mg/kg(max)
Note 1:0-Aminoazotoluene(CAS NO.97-56-3)is further reduced to o-toluidine (CAS NO.95-53-4)and quantifled by this.
Note 2:5-Nltro-o-toluidine(CAS NO.99-55-8)is further reduced to 4-Methyl-m-phenylene diamine(CAS NO.95-80-7)and quantifired by this.
Note 3:4-Amino-azobenzene(CAS NO.60-09-3)is detected as p-Phenylenediamine and aniline,When p-phenylendiamine and Aniline are detected in one sample simultaneousty is this an-indisation that the banned 4-Amine-azobenzene(CAS NO,60-09-3)may be contained An additional analysis is performed to confirm and measure by §64 LFGB B 82-0209
Pass:According to the analysis as carned out,AZO colorants,which release the listed aromatic amines under Directive 2002/61/EC,were less than 150 mg/kg.
EN71-Part 3:Migration of certain elements\x05\x05\x05
Test method:Soluble toxic element contents are determined by lnductively Coupled Plasma-Optical Emission Spectrometry (ICP-OES)\x05\x05\x05
EN71-3,Toys safety ,1994+A1;2000+AC;2000+AC:2002\x05\x05\x05
Limit:EN71-3,See below\x05\x05\x05
8.9 For Paints,including,varnishes,lacquers,glazing powders and similar materials in solid or in liquid form
Remark:
Detection limit:2.5 mg/kg for each of the 8 soluble toxic elements
Sol:Soluble
1:AS the malenal under test is not in the test scope of EN71,however ,required by the applicant,we have adopted the test method of EN 71-3,1994+A1+AC,clause 8.9 to perform the above test and get the conclusion refer to EN 71-3
Maine test instruments used for this method:\x05\x05
lnstrument\x05Manufactory\x05Model/Type
ICP-OES\x05 PerkinElmer 5300DV
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